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1 M, [APS]/[An] = 1:1; [Fe 2(SO4)3]/ [An] = 3:1; reaction time :15 h, reaction temperature : 0~5oC. In principle, aniline monomer can be regarded as amphiphilic molecule due to its hydrophobic group of benzene ring and hydrophilic -NH2 group. As a result, the micelle composed of aniline monomer is expected to be existence in either homogenous or heterogeneous polymerization. The micelles can be served as the soft-templates in the formation of the PANI nanofibers prepared by TFMDF. Once adding the oxidant, the polymerization takes place at the 38 Hang-Jun Ding, Yun-Ze Long, Zhi-Ming Zhang et al.

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42 Hang-Jun Ding, Yun-Ze Long, Zhi-Ming Zhang et al. Figure 10. SEM images of (a) PANI-SA spheres deposited on the silicon wafer and (b) silicon wafer; (c) PANI-SA spheres deposited on the PTFE modified glass substrate and (b) PTFE modified glass substrate. 4 mm/s; polymerization time: 30 min. Mono-dispersed PANI micro-spheres with 300~400 nm in diameter deposed on the glass substrate were successfully prepared, as shown in Figure 10. Based on the micelles modal [60], micelles composed of aniline and SA might acts a soft-template in the formation of the spheres deposited on the substrates due to its hydrophilic –OH and –NH groups and hydrophobic benzene ring groups.

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